Synthesis, Characterization and Fluorimetric Studies of a New Quinoline Based Schiff Base Using for Detection Al3

Meliha Kutluca Alıcı

Makale detayları

Synthesis, Characterization and Fluorimetric Studies of a New Quinoline Based Schiff Base Using for Detection Al3

Yazarlar:

Meliha Kutluca Alıcı

Yayıncı:

Afyon Kocatepe University

Ana Başlıklar:

İnorganik Kimya (Diğer)

Dergi:

Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.25 Issue 3, pp.471-476

Belge Tipi:

Makale

Yayın Tarihi:

10/2025

Belge Dili:

Türkçe

Document ID (Org No.):

2001348305

pISSN:

2149-3367

Anahtar kelimeler:

Özet:

 In this study, firstly, the synthesis of Schiff base HQ-BT compound to be used as a fluorescence sensor was carried out and its chemical structure was verified 1H-NMR ve 13C-NMR. It was then found that the new HQ-BT compound gave a significant fluorescence emission about 100-fold increase only towards Al3 metal among the metal ions used. As a result of the studies, it was determined that the new HQ-BT compound complexed with Al3 metal in a 1:1 ratio. It was also found that HQ-BT compound has a low detection of limit as 2.91 µM against Al3 metal ions.

 In this study, firstly, the synthesis of Schiff base HQ-BT compound to be used as a fluorescence sensor was carried out and its chemical structure was verified 1H-NMR ve 13C-NMR. It was then found that the new HQ-BT compound gave a significant fluorescence emission about 100-fold increase only towards Al3 metal among the metal ions used. As a result of the studies, it was determined that the new HQ-BT compound complexed with Al3 metal in a 1:1 ratio. It was also found that HQ-BT compound has a low detection of limit as 2.91 µM against Al3 metal ions.

 In this study, firstly, the synthesis of Schiff base HQ-BT compound to be used as a fluorescence sensor was carried out and its chemical structure was verified 1H-NMR ve 13C-NMR. It was then found that the new HQ-BT compound gave a significant fluorescence emission about 100-fold increase only towards Al3 metal among the metal ions used. As a result of the studies, it was determined that the new HQ-BT compound complexed with Al3 metal in a 1:1 ratio. It was also found that HQ-BT compound has a low detection of limit as 2.91 µM against Al3 metal ions.

 Bu çalışmada ilk olarak fluoresans sensör olarak kullanılacak Schiff bazı HQ-BT bileşiğinin sentezi gerçekleştirilmiş ve kimyasal yapısı doğrulanmıştır 1H-NMR ve 13C-NMR. Daha sonra yeni HQ-BT bileşiğinin kullanılan metal iyonları içerisinde sadece Al3 metaline karşı ciddi derecede bir fluoresans emisyon yaklaşık 100 kat artış verdiği tespit edilmiştir. Bununla beraber yapılan çalışmalar sonucunda yeni HQ-BT bileşiği ile Al3 metalinin 1:1 oranında kompleksleşme yaptığı tespit edilmiştir. Ayrıca HQ-BT bileşiğinin Al3 metal iyonlarına karşı 2.91 µM gibi düşük bir tespit limitine sahip olduğu bulunmuştur.

Makale detayları

Synthesis, Characterization and Fluorimetric Studies of a New Quinoline Based Schiff Base Using for Detection Al3

Yazarlar:

Meliha Kutluca Alıcı

Yayıncı:

Afyon Kocatepe University

Ana Başlıklar:

İnorganik Kimya (Diğer)

Dergi:

Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.25 Issue 3, pp.471-476

Belge Tipi:

Makale

Yayın Tarihi:

10/2025

Belge Dili:

Türkçe

Document ID (Org No.):

2001348305

pISSN:

2149-3367

Fluorescence sensor

Al3+

Schiff base

NMRFluoresans sensör

Al3+

Schiff bazı

NMR

Sayı

Makale detayları

Yazarlar: Meliha Kutluca Alıcı

Yayıncı: Afyon Kocatepe University

Ana Başlıklar: İnorganik Kimya (Diğer)

Dergi: Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.25 Issue 3, pp.471-476

Belge Tipi: Makale

Yayın Tarihi: 10/2025

Belge Dili: Türkçe

Document ID (Org No.): 2001348305

pISSN: 2149-3367

Sayı

Yazarlar:

Meliha Kutluca Alıcı

Yayıncı:

Afyon Kocatepe University

Ana Başlıklar:

İnorganik Kimya (Diğer)

Dergi:

Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.25 Issue 3, pp.471-476

Belge Tipi:

Makale

Yayın Tarihi:

10/2025

Belge Dili:

Türkçe

Document ID (Org No.):

2001348305

pISSN:

2149-3367