Synthesis of Metal Complexes of Some Formazans Obtaining From Cinnamaldehyde and Investigation of Their Dyeing Properties Using Different Methods

Nursabah SARIKAVAKLI; Fatma EROL

doi:https://doi.org/10.31590/ejosat.442722

Makale detayları

Synthesis of Metal Complexes of Some Formazans Obtaining From Cinnamaldehyde and Investigation of Their Dyeing Properties Using Different Methods

Yazarlar:

Nursabah SARIKAVAKLI | Fatma EROL

Yayıncı:

Osman SAĞDIÇ

Ana Başlıklar:

Uygulamalı fizik

Dergi:

European Journal of Science and Technology 2018 Vol. Issue 14, pp.315-322

Belge Tipi:

Makale

Yayın Tarihi:

12/2018

Belge Dili:

İngilizce

Document ID (Org No.):

2000920303

Sıklık:

Üç Aylık

eISSN:

2148-2683

DOI:

https://doi.org/10.31590/ejosat.442722

Anahtar kelimeler:

Özet:

 


In this study, two formazans were synthesized by coupling cinnamaldehyde phenyl hydrazone which was obtained by activation of cinnamaldehyde with phenylhydrazone, with diazonium salts of anthranilic acid and sulfonilic acid. The complexes of Co+2, Ni+2, Cu2+ salts of these formazans were also synthesized. These compounds were characterized by elemental analysis, infrared (IR), ultraviolet–visible (UV–vis),1H nuclear magnetic resonance (1H-NMR) and  13C-NMR spectra datas. Investigation of availability of these compounds as dyes were carried out for this purpose. In the present experimental approach, we applied two methods; The first one was direct dyeing with these complexes, and the other one was complex formation on the fibres. Finally, an investigation was carried out  for the fastness values (test) and it was found higher values, which was quite better and different from the other workers / researcher working in the same field.

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In this study,
two formazans were synthesized by coupling cinnamaldehyde phenyl hydrazone
which was obtained by activation of cinnamaldehyde with phenylhydrazone, with
diazonium salts of anthranilic acid and sulfonilic acid. The complexes of Co+2,
Ni+2, Cu2+ salts of these formazans were also
synthesized. These compounds were characterized by elemental analysis, infrared
(IR), ultraviolet–visible (UV–vis),1H nuclear magnetic resonance (1H-NMR) and  13C-NMR spectra datas. Investigation of availability of
these compounds as dyes were
carried out for this purpose. In the present experimental approach, we
applied two methods; The first one was direct dyeing with these complexes, and
the other one was complex formation on the fibres. Finally, an
investigation was carried out  for the fastness
values (test) and it was found higher values, which was quite better and
different from the other workers / researcher working in the same field.



.

Makale detayları

Synthesis of Metal Complexes of Some Formazans Obtaining From Cinnamaldehyde and Investigation of Their Dyeing Properties Using Different Methods

Yazarlar:

Nursabah SARIKAVAKLI | Fatma EROL

Yayıncı:

Osman SAĞDIÇ

Ana Başlıklar:

Uygulamalı fizik

Dergi:

European Journal of Science and Technology 2018 Vol. Issue 14, pp.315-322

Belge Tipi:

Makale

Yayın Tarihi:

12/2018

Belge Dili:

İngilizce

Document ID (Org No.):

2000920303

Sıklık:

Üç Aylık

eISSN:

2148-2683

DOI:

https://doi.org/10.31590/ejosat.442722

Formazans

Metal complexes

Dyeing

Fastness properties

Sayı

Makale detayları

Synthesis of Metal Complexes of Some Formazans Obtaining From Cinnamaldehyde and Investigation of Their Dyeing Properties Using Different Methods

Yazarlar: Nursabah SARIKAVAKLI | Fatma EROL

Yayıncı: Osman SAĞDIÇ

Ana Başlıklar: Uygulamalı fizik

Dergi: European Journal of Science and Technology 2018 Vol. Issue 14, pp.315-322

Belge Tipi: Makale

Yayın Tarihi: 12/2018

Belge Dili: İngilizce

Document ID (Org No.): 2000920303

Sıklık: Üç Aylık

eISSN: 2148-2683

DOI: https://doi.org/10.31590/ejosat.442722

Formazans

Metal complexes

Dyeing

Fastness properties

Sayı

Yazarlar:

Nursabah SARIKAVAKLI | Fatma EROL

Yayıncı:

Osman SAĞDIÇ

Ana Başlıklar:

Uygulamalı fizik

Dergi:

European Journal of Science and Technology 2018 Vol. Issue 14, pp.315-322

Belge Tipi:

Makale

Yayın Tarihi:

12/2018

Belge Dili:

İngilizce

Document ID (Org No.):

2000920303

Sıklık:

Üç Aylık

eISSN:

2148-2683

DOI:

https://doi.org/10.31590/ejosat.442722