Chelating agent free solid phase extraction (CAF-SPE) method for separation and/or preconcentration of iron(III) ions

Chelating agent free solid phase extract For

Makale detayları

Chelating agent free solid phase extraction (CAF-SPE) method for separation and/or preconcentration of iron(III) ions

Yazarlar:

Chelating agent free solid phase extract For

Yayıncı:

TUBITAK

Dergi:

Turkish Journal of Chemistry 2010 Vol.34 Issue 2, pp.207-218

Belge Tipi:

Makale

Yayın Tarihi:

1/2010

Belge Dili:

Türkçe

Document ID (Org No.):

2000728094

Sıklık:

İki Aylık

eISSN:

1303-6130

pISSN:

1300-0527

Özet:

 

This paper presents a chelating agent free solid phase  extraction (CAF-SPE) method for the separation and/or preconcentration  of trace iron(III) ions.  This method is based on the sorption of  Fe(III) ions without using any chelating agent onto Amberlyst 36  resin.  A good relative standard deviation (3%), high recovery  (>95%), high enrichment factor (100), and low detection limit (0.32  m g L-1) were obtained.  The adsorption capacity of resin was 117  mg g-1 for iron(III).  The method was applied for the determination  of iron various in water and commercial tea bag samples.  The accuracy  of the method was confirmed by analyzing Certified Reference Material  (GBW 07605).

 

This paper presents a chelating agent free solid phase  extraction (CAF-SPE) method for the separation and/or preconcentration  of trace iron(III) ions.  This method is based on the sorption of  Fe(III) ions without using any chelating agent onto Amberlyst 36  resin.  A good relative standard deviation (3%), high recovery  (>95%), high enrichment factor (100), and low detection limit (0.32  m g L-1) were obtained.  The adsorption capacity of resin was 117  mg g-1 for iron(III).  The method was applied for the determination  of iron various in water and commercial tea bag samples.  The accuracy  of the method was confirmed by analyzing Certified Reference Material  (GBW 07605).

Makale detayları

Chelating agent free solid phase extraction (CAF-SPE) method for separation and/or preconcentration of iron(III) ions

Yazarlar: Chelating agent free solid phase extract For

Yayıncı: TUBITAK

Dergi: Turkish Journal of Chemistry 2010 Vol.34 Issue 2, pp.207-218

Belge Tipi: Makale

Yayın Tarihi: 1/2010

Belge Dili: Türkçe

Document ID (Org No.): 2000728094

Sıklık: İki Aylık

eISSN: 1303-6130

pISSN: 1300-0527

Sayı

Yazarlar:

Chelating agent free solid phase extract For

Yayıncı:

TUBITAK

Dergi:

Turkish Journal of Chemistry 2010 Vol.34 Issue 2, pp.207-218

Belge Tipi:

Makale

Yayın Tarihi:

1/2010

Belge Dili:

Türkçe

Document ID (Org No.):

2000728094

Sıklık:

İki Aylık

eISSN:

1303-6130

pISSN:

1300-0527