Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography

Tuğçe Unutkan Gösterişli

Makale detayları

Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography

Yazarlar:

Tuğçe Unutkan Gösterişli

Yayıncı:

Sakarya University

Ana Başlıklar:

Analytical Chemistry (Other)

Dergi:

Sakarya University Journal of Science Vol.27 Issue 5, pp.1002-1007

Belge Tipi:

Makale

Yayın Tarihi:

10/2023

Belge Dili:

İngilizce

Document ID (Org No.):

2001300450

pISSN:

2147-835X

Anahtar kelimeler:

Özet:

 In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer 50.0 mM, pH 4.0:acetonitrile 55:45 vv as mobile phase. Under the optimal conditions, the limits of detection and quantification LOD and LOQ were found as 7.4  24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable  recoveries in the range of 81.4112.9, while the values of relative standard deviation RSD were below 10 showing a satisfactory applicability for cymoxanil in such complex real samples matrix.

 In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer 50.0 mM, pH 4.0:acetonitrile 55:45 vv as mobile phase. Under the optimal conditions, the limits of detection and quantification LOD and LOQ were found as 7.4  24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable  recoveries in the range of 81.4112.9, while the values of relative standard deviation RSD were below 10 showing a satisfactory applicability for cymoxanil in such complex real samples matrix.

 In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer 50.0 mM, pH 4.0:acetonitrile 55:45 vv as mobile phase. Under the optimal conditions, the limits of detection and quantification LOD and LOQ were found as 7.4  24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable  recoveries in the range of 81.4112.9, while the values of relative standard deviation RSD were below 10 showing a satisfactory applicability for cymoxanil in such complex real samples matrix.

 In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer 50.0 mM, pH 4.0:acetonitrile 55:45 vv as mobile phase. Under the optimal conditions, the limits of detection and quantification LOD and LOQ were found as 7.4  24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable  recoveries in the range of 81.4112.9, while the values of relative standard deviation RSD were below 10 showing a satisfactory applicability for cymoxanil in such complex real samples matrix.

Makale detayları

Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography

Yazarlar:

Tuğçe Unutkan Gösterişli

Yayıncı:

Sakarya University

Ana Başlıklar:

Analytical Chemistry (Other)

Dergi:

Sakarya University Journal of Science Vol.27 Issue 5, pp.1002-1007

Belge Tipi:

Makale

Yayın Tarihi:

10/2023

Belge Dili:

İngilizce

Document ID (Org No.):

2001300450

pISSN:

2147-835X

Cymoxanil

potato flour

high performance liquid chromatography

fungidice

Sayı

Makale detayları

Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography

Yazarlar: Tuğçe Unutkan Gösterişli

Yayıncı: Sakarya University

Ana Başlıklar: Analytical Chemistry (Other)

Dergi: Sakarya University Journal of Science Vol.27 Issue 5, pp.1002-1007

Belge Tipi: Makale

Yayın Tarihi: 10/2023

Belge Dili: İngilizce

Document ID (Org No.): 2001300450

pISSN: 2147-835X

Cymoxanil

potato flour

high performance liquid chromatography

fungidice

Sayı

Yazarlar:

Tuğçe Unutkan Gösterişli

Yayıncı:

Sakarya University

Ana Başlıklar:

Analytical Chemistry (Other)

Dergi:

Sakarya University Journal of Science Vol.27 Issue 5, pp.1002-1007

Belge Tipi:

Makale

Yayın Tarihi:

10/2023

Belge Dili:

İngilizce

Document ID (Org No.):

2001300450

pISSN:

2147-835X