EASY SYNTHESIS OF 3,4-DIHYDROPYRIMIDIN -2-(1H)-ONES USING PHOSPHATE FERTILIZERS MAP, DAP AND TSP AS EFFICIENT CATALYSTS

Sarra SIBOUS; Said BOUKHRIS; Rachida GHAILANE; Nouzha HABBADI; Amina HASSIKOU; Abdelaziz SOUIZI

doi:https://doi.org/10.18596/jotcsa.286900

Makale detayları

EASY SYNTHESIS OF 3,4-DIHYDROPYRIMIDIN -2-(1H)-ONES USING PHOSPHATE FERTILIZERS MAP, DAP AND TSP AS EFFICIENT CATALYSTS

Yazarlar:

Sarra SIBOUS | Said BOUKHRIS | Rachida GHAILANE | Nouzha HABBADI | Amina HASSIKOU | Abdelaziz SOUIZI

Yayıncı:

Turkish Chemical Society

Ana Başlıklar:

Kimya mühendisliği

Dergi:

Journal of the Turkish Chemical Society Section A: Chemistry 2017 Vol.4 Issue 2, pp.481-488

Belge Tipi:

Makale

Yayın Tarihi:

3/2017

Belge Dili:

İngilizce

Document ID (Org No.):

2000503545

Sıklık:

Üç Aylık

eISSN:

2149-0120

DOI:

https://doi.org/10.18596/jotcsa.286900

Özet:

 


A simple,
efficient and green procedure has been developed for the synthesis of
dihydropyrimidinones (Products of Biginelli) using phosphate fertilizers (mono-ammonium
phosphate (MAP), di-ammonium phosphate (DAP) and triple super phosphate (TSP))
as catalyst. The one-step reaction involved the three compounds, which are
registered aromatic aldehydes, dicarbonyl compounds and the urea/thiourea. This
new method provides some advantages such as obtaining excellent yields (98%),
as well as the short duration of the reaction, which may attain 2 min. These
catalytic heterogeneous systems present also the advantage of being easily
recycled.


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Makale detayları

EASY SYNTHESIS OF 3,4-DIHYDROPYRIMIDIN -2-(1H)-ONES USING PHOSPHATE FERTILIZERS MAP, DAP AND TSP AS EFFICIENT CATALYSTS

Yazarlar: Sarra SIBOUS | Said BOUKHRIS | Rachida GHAILANE | Nouzha HABBADI | Amina HASSIKOU | Abdelaziz SOUIZI

Yayıncı: Turkish Chemical Society

Ana Başlıklar: Kimya mühendisliği

Dergi: Journal of the Turkish Chemical Society Section A: Chemistry 2017 Vol.4 Issue 2, pp.481-488

Belge Tipi: Makale

Yayın Tarihi: 3/2017

Belge Dili: İngilizce

Document ID (Org No.): 2000503545

Sıklık: Üç Aylık

eISSN: 2149-0120

DOI: https://doi.org/10.18596/jotcsa.286900

Sayı

Yazarlar:

Sarra SIBOUS | Said BOUKHRIS | Rachida GHAILANE | Nouzha HABBADI | Amina HASSIKOU | Abdelaziz SOUIZI

Yayıncı:

Turkish Chemical Society

Ana Başlıklar:

Kimya mühendisliği

Dergi:

Journal of the Turkish Chemical Society Section A: Chemistry 2017 Vol.4 Issue 2, pp.481-488

Belge Tipi:

Makale

Yayın Tarihi:

3/2017

Belge Dili:

İngilizce

Document ID (Org No.):

2000503545

Sıklık:

Üç Aylık

eISSN:

2149-0120

DOI:

https://doi.org/10.18596/jotcsa.286900