Influence Of Graphene Oxide Amount on The Structure and Morphology of In2O3-Reduced Graphene Oxide Composite Film

Hülya Öztürk Doğan; Mertcan Sezgin

Makale detayları

Influence Of Graphene Oxide Amount on The Structure and Morphology of In2O3-Reduced Graphene Oxide Composite Film

Yazarlar:

Hülya Öztürk Doğan | Mertcan Sezgin

Yayıncı:

Igdir University

Ana Başlıklar:

Elektroanalitik Kimya | Elektrokimyasal Teknolojiler

Dergi:

Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.15 Issue 2, pp.615-623

Belge Tipi:

Makale

Yayın Tarihi:

1/2025

Belge Dili:

İngilizce

Document ID (Org No.):

2001345221

pISSN:

2536-4618

Anahtar kelimeler:

Özet:

 In this study, indium oxide-reduced graphene oxide In2O3-rGO composites were produced in one-pot using an electrochemical technique for the first time. The effect of graphene oxide GO amount on the composition and morphology of the composite structure was investigated. For this purpose, electrolyte solutions containing GO and In3 ions were mixed at different volume ratios. Deposits were carried out at constant potential in different electrolyte compositions. The characterizations of the composite structures prepared under different experimental parameters were investigated using X-ray diffraction spectroscopy XRD, X-ray photoelectron spectroscopy XPS, Raman spectroscopy, and field effect scanning electron microscopy FESEM techniques. It was concluded that the In2O3-rGO composite with the best composition was obtained in 1:1 GO: In3 electrolyte by volume.

 In this study, indium oxide-reduced graphene oxide In2O3-rGO composites were produced in one-pot using an electrochemical technique for the first time. The effect of graphene oxide GO amount on the composition and morphology of the composite structure was investigated. For this purpose, electrolyte solutions containing GO and In3 ions were mixed at different volume ratios. Deposits were carried out at constant potential in different electrolyte compositions. The characterizations of the composite structures prepared under different experimental parameters were investigated using X-ray diffraction spectroscopy XRD, X-ray photoelectron spectroscopy XPS, Raman spectroscopy, and field effect scanning electron microscopy FESEM techniques. It was concluded that the In2O3-rGO composite with the best composition was obtained in 1:1 GO: In3 electrolyte by volume.

 In this study, indium oxide-reduced graphene oxide In2O3-rGO composites were produced in one-pot using an electrochemical technique for the first time. The effect of graphene oxide GO amount on the composition and morphology of the composite structure was investigated. For this purpose, electrolyte solutions containing GO and In3 ions were mixed at different volume ratios. Deposits were carried out at constant potential in different electrolyte compositions. The characterizations of the composite structures prepared under different experimental parameters were investigated using X-ray diffraction spectroscopy XRD, X-ray photoelectron spectroscopy XPS, Raman spectroscopy, and field effect scanning electron microscopy FESEM techniques. It was concluded that the In2O3-rGO composite with the best composition was obtained in 1:1 GO: In3 electrolyte by volume.

 Bu çalışmada, elektrokimyasal bir teknik kullanılarak ilk defa tek kapta indiyum oksitle indirgenmiş grafen oksit In2O3-rGO kompozitleri üretildi. Grafen oksit GO miktarının kompozit yapının kompozisyonu ve morfolojisi üzerindeki etkisi incelendi. Bu amaçla, GO ve In3 iyonları içeren elektrolit çözeltileri farklı hacim oranlarında karıştırıldı. Biriktirmeler farklı elektrolit kompozisyonlarında sabit potansiyelde gerçekleştirildi. Farklı deneysel parametreler altında hazırlanan kompozit yapıların karakterizasyonları X-ışını kırınım spektroskopisi XRD, X-ışını fotoelektron spektroskopisi XPS, Raman spektroskopisi ve alan etkili taramalı elektron mikroskobu FESEM teknikleri kullanılarak incelendi. En iyi kompozisyona sahip In2O3-rGO kompozitinin hacimce 1:1 GO:In3 elektrolit oranında elde edildiği sonucuna varıldı.

Makale detayları

Influence Of Graphene Oxide Amount on The Structure and Morphology of In2O3-Reduced Graphene Oxide Composite Film

Yazarlar:

Hülya Öztürk Doğan | Mertcan Sezgin

Yayıncı:

Igdir University

Ana Başlıklar:

Elektroanalitik Kimya | Elektrokimyasal Teknolojiler

Dergi:

Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.15 Issue 2, pp.615-623

Belge Tipi:

Makale

Yayın Tarihi:

1/2025

Belge Dili:

İngilizce

Document ID (Org No.):

2001345221

pISSN:

2536-4618

• Electrochemical deposition

• Indium oxide

• Nanocomposite

• Reduced graphene oxide• Elektrokimyasal depozisyon

• İndiyum oksit

• Nanokompozit

• İndirgenmiş grafen oksit

Sayı

Makale detayları

Yazarlar: Hülya Öztürk Doğan | Mertcan Sezgin

Yayıncı: Igdir University

Ana Başlıklar: Elektroanalitik Kimya | Elektrokimyasal Teknolojiler

Dergi: Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.15 Issue 2, pp.615-623

Belge Tipi: Makale

Yayın Tarihi: 1/2025

Belge Dili: İngilizce

Document ID (Org No.): 2001345221

pISSN: 2536-4618

Sayı

Yazarlar:

Hülya Öztürk Doğan | Mertcan Sezgin

Yayıncı:

Igdir University

Ana Başlıklar:

Elektroanalitik Kimya | Elektrokimyasal Teknolojiler

Dergi:

Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.15 Issue 2, pp.615-623

Belge Tipi:

Makale

Yayın Tarihi:

1/2025

Belge Dili:

İngilizce

Document ID (Org No.):

2001345221

pISSN:

2536-4618