A comparative study on fabrication of Cu22_{2}ZnSnS44_{4} (CZTS) nanofibers using acetate and chloride metal precursors

BURAK ZAFER BÜYÜKBEKAR; FARUK ÖZEL; HÜSEYİN ŞAKALAK; HALİT ÇAVUŞOĞLU; MUSTAFA ERSÖZ; MAHMUT KUŞ; MUSTAFA SELMAN YAVUZ

Makale detayları

A comparative study on fabrication of Cu22_{2}ZnSnS44_{4} (CZTS) nanofibers using acetate and chloride metal precursors

Yazarlar:

BURAK ZAFER BÜYÜKBEKAR | FARUK ÖZEL | HÜSEYİN ŞAKALAK | HALİT ÇAVUŞOĞLU | MUSTAFA ERSÖZ | MAHMUT KUŞ | MUSTAFA SELMAN YAVUZ

Yayıncı:

TUBITAK

Dergi:

Turkish Journal of Chemistry 2015 Vol.39 Issue 4, pp.897-903

Belge Tipi:

Makale

Yayın Tarihi:

8/2015

Belge Dili:

Türkçe

Document ID (Org No.):

2000726844

Sıklık:

İki Aylık

eISSN:

1303-6130

pISSN:

1300-0527

Özet:

 

This study reports, for the first time, the fabrication of electrospun Cu22_{2}ZnSnS44_{4} (CZTS) nanofibers using metal acetate precursors. Viscous poly(vinyl pyrrolidone) (PVP) solution containing acetate or chloride salts of copper, zinc, and tin was electrospun onto a conductive substrate. The PVP nanofibers that have a mixture of metal salts were annealed at elevated temperatures. After calcination, these nanofibers were treated with the sulfur source and then annealed again in order to generate CZTS nanofibers. The CZTS nanofibers generated from acetate and chloride salts were characterized and compared. Belt-like and wire-like nanofibers were obtained when using metal acetate and chloride precursors, respectively.

 

This study reports, for the first time, the fabrication of electrospun Cu22_{2}ZnSnS44_{4} (CZTS) nanofibers using metal acetate precursors. Viscous poly(vinyl pyrrolidone) (PVP) solution containing acetate or chloride salts of copper, zinc, and tin was electrospun onto a conductive substrate. The PVP nanofibers that have a mixture of metal salts were annealed at elevated temperatures. After calcination, these nanofibers were treated with the sulfur source and then annealed again in order to generate CZTS nanofibers. The CZTS nanofibers generated from acetate and chloride salts were characterized and compared. Belt-like and wire-like nanofibers were obtained when using metal acetate and chloride precursors, respectively.

Makale detayları

A comparative study on fabrication of Cu22_{2}ZnSnS44_{4} (CZTS) nanofibers using acetate and chloride metal precursors

Yazarlar: BURAK ZAFER BÜYÜKBEKAR | FARUK ÖZEL | HÜSEYİN ŞAKALAK | HALİT ÇAVUŞOĞLU | MUSTAFA ERSÖZ | MAHMUT KUŞ | MUSTAFA SELMAN YAVUZ

Yayıncı: TUBITAK

Dergi: Turkish Journal of Chemistry 2015 Vol.39 Issue 4, pp.897-903

Belge Tipi: Makale

Yayın Tarihi: 8/2015

Belge Dili: Türkçe

Document ID (Org No.): 2000726844

Sıklık: İki Aylık

eISSN: 1303-6130

pISSN: 1300-0527

Sayı

Yazarlar:

BURAK ZAFER BÜYÜKBEKAR | FARUK ÖZEL | HÜSEYİN ŞAKALAK | HALİT ÇAVUŞOĞLU | MUSTAFA ERSÖZ | MAHMUT KUŞ | MUSTAFA SELMAN YAVUZ

Yayıncı:

TUBITAK

Dergi:

Turkish Journal of Chemistry 2015 Vol.39 Issue 4, pp.897-903

Belge Tipi:

Makale

Yayın Tarihi:

8/2015

Belge Dili:

Türkçe

Document ID (Org No.):

2000726844

Sıklık:

İki Aylık

eISSN:

1303-6130

pISSN:

1300-0527