The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride

Fatma Tuğçe ŞENBERBER

doi:https://doi.org/10.21541/apjes.382382

Makale detayları

The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride

Yazarlar:

Fatma Tuğçe ŞENBERBER

Yayıncı:

Akademik Perspektif Derneği

Ana Başlıklar:

Uygulamalı fizik

Dergi:

Academic Platform - Journal of Engineering and Science 2018 Vol.6 Issue 3, pp.92-96

Belge Tipi:

Makale

Yayın Tarihi:

9/2018

Belge Dili:

İngilizce

Document ID (Org No.):

2000874872

Sıklık:

Aylık

eISSN:

2822-2385

DOI:

https://doi.org/10.21541/apjes.382382

Anahtar kelimeler:

Özet:

 


In this study, the synthesis and characterization of
potassium borate were studied using KCl, NaOH and H3BO3 asthe starting materials. The effects of the boron precursor, reaction
temperature and time on the structure of the synthesized potassium borate were
investigated. X-ray diffraction (XRD) showed the synthesized sample was
santite, which has the chemical formula KB5O84H2O (Powder diffraction file number:
01-1072-1688). The XRD scores increased upon decreasing the reaction
temperature and time. The characteristic band values observed for boron and
oxygen were investigated using Fourier transform infrared (FT-IR) and Raman
spectroscopy. The morphology of the synthesized samples was characterized using
scanning electron microscopy (SEM). The samples were found to be on the
micro-scale with particle sizes <2.54 µm. The reaction yields were in the
range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.

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In this study, the synthesis and characterization of potassium borate were studied using KCl, NaOH and H3BO3 asthe starting materials. The effects of the boron precursor, reaction temperature and time on the structure of the synthesized potassium borate were investigated. X-ray diffraction (XRD) showed the synthesized sample was santite, which has the chemical formula KB5O84H2O (Powder diffraction file number: 01-1072-1688). The XRD scores increased upon decreasing the reaction temperature and time. The characteristic band values observed for boron and oxygen were investigated using Fourier transform infrared (FT-IR) and Raman spectroscopy. The morphology of the synthesized samples was characterized using scanning electron microscopy (SEM). The samples were found to be on the micro-scale with particle sizes <2.54 µm. The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.


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Makale detayları

The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride

Yazarlar:

Fatma Tuğçe ŞENBERBER

Yayıncı:

Akademik Perspektif Derneği

Ana Başlıklar:

Uygulamalı fizik

Dergi:

Academic Platform - Journal of Engineering and Science 2018 Vol.6 Issue 3, pp.92-96

Belge Tipi:

Makale

Yayın Tarihi:

9/2018

Belge Dili:

İngilizce

Document ID (Org No.):

2000874872

Sıklık:

Aylık

eISSN:

2822-2385

DOI:

https://doi.org/10.21541/apjes.382382

spektroskopi

SEM

XRD

Hidrotermal senztez

potayum borat

Sayı

Makale detayları

The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride

Yazarlar: Fatma Tuğçe ŞENBERBER

Yayıncı: Akademik Perspektif Derneği

Ana Başlıklar: Uygulamalı fizik

Dergi: Academic Platform - Journal of Engineering and Science 2018 Vol.6 Issue 3, pp.92-96

Belge Tipi: Makale

Yayın Tarihi: 9/2018

Belge Dili: İngilizce

Document ID (Org No.): 2000874872

Sıklık: Aylık

eISSN: 2822-2385

DOI: https://doi.org/10.21541/apjes.382382

spektroskopi

SEM

XRD

Hidrotermal senztez

potayum borat

Sayı

Yazarlar:

Fatma Tuğçe ŞENBERBER

Yayıncı:

Akademik Perspektif Derneği

Ana Başlıklar:

Uygulamalı fizik

Dergi:

Academic Platform - Journal of Engineering and Science 2018 Vol.6 Issue 3, pp.92-96

Belge Tipi:

Makale

Yayın Tarihi:

9/2018

Belge Dili:

İngilizce

Document ID (Org No.):

2000874872

Sıklık:

Aylık

eISSN:

2822-2385

DOI:

https://doi.org/10.21541/apjes.382382