Optimization of the Schiff-Base Reaction of Acetylacetone with Biogenic Amines

Bediha AKMESE; Asan ADEM

doi:https://doi.org/10.17350/HJSE19030000052

Makale detayları

Optimization of the Schiff-Base Reaction of Acetylacetone with Biogenic Amines

Yazarlar:

Bediha AKMESE | Asan ADEM

Yayıncı:

Hitit University

Dergi:

Hittite Journal of Science and Engineering 2017 Vol.4 Issue 1, pp.79-83

Belge Tipi:

Makale

Yayın Tarihi:

6/2017

Belge Dili:

İngilizce

Document ID (Org No.):

2000451840

Sıklık:

Üç Aylık

eISSN:

2148-4171

DOI:

https://doi.org/10.17350/HJSE19030000052

Özet:

 

I n this work, optimum conditions for the derivatization reaction of biogenic amines  histamine, tyramine, putrecine, tryptamine, phenylethylamine, cadaverine, spermidine and spermine  with acetylacetone have been determined. In this reaction, the amount of K2HPO4, reaction time, reagent amount, solvent choice and solvent amount were optimized. As a result of this study, optimum conditions were determined as amount of K2HPO4 2 g, reaction time 20 min, amount of acetylacetone 1 mL, solvent methanol and amount of solvent 10 mL.

Makale detayları

Optimization of the Schiff-Base Reaction of Acetylacetone with Biogenic Amines

Yazarlar: Bediha AKMESE | Asan ADEM

Yayıncı: Hitit University

Dergi: Hittite Journal of Science and Engineering 2017 Vol.4 Issue 1, pp.79-83

Belge Tipi: Makale

Yayın Tarihi: 6/2017

Belge Dili: İngilizce

Document ID (Org No.): 2000451840

Sıklık: Üç Aylık

eISSN: 2148-4171

DOI: https://doi.org/10.17350/HJSE19030000052

Sayı

Yazarlar:

Bediha AKMESE | Asan ADEM

Yayıncı:

Hitit University

Dergi:

Hittite Journal of Science and Engineering 2017 Vol.4 Issue 1, pp.79-83

Belge Tipi:

Makale

Yayın Tarihi:

6/2017

Belge Dili:

İngilizce

Document ID (Org No.):

2000451840

Sıklık:

Üç Aylık

eISSN:

2148-4171

DOI:

https://doi.org/10.17350/HJSE19030000052