Microencapsulation and Characterization Studies of Brassica oleracea var. capitata L. (Cabbage) Plant Extract Using Response Surface Methodology

Elif Köksal; Fethiye Göde

Makale detayları

Microencapsulation and Characterization Studies of Brassica oleracea var. capitata L. (Cabbage) Plant Extract Using Response Surface Methodology

Yazarlar:

Elif Köksal | Fethiye Göde

Yayıncı:

Afyon Kocatepe University

Ana Başlıklar:

Mühendislik

Dergi:

Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.24 Issue 1, pp.14-22

Belge Tipi:

Makale

Yayın Tarihi:

2/2024

Belge Dili:

Türkçe

Document ID (Org No.):

2001312333

pISSN:

2149-3367

Anahtar kelimeler:

Özet:

 In our study, cabbage plant extract containing the active ingredient S-methylmethionine vitamin U was successfully microencapsulated by complex coacervation method using two different natural polymeric wall materials consisting of Gelatin-Gum Arabic GE-GA and Gelatin-Sodium alginate GE-SA. A response surface methodology RSM was used to optimize the encapsulation efficiency conditions. The encapsulation efficiency of the microencapsulated cabbage extract was investigated using different polymers in terms of two variables: the amount of core material g and the amount of crosslinker mL. The highest yields obtained as a result of the experiments were 67.72 for gelatin-gum arabic and 54.68 for gelatin-sodium alginate. The morphological structures of the microcapsules with the highest efficiency were examined by optical microscope and scanning electron microscope SEM. The Fourier transform infrared spectroscopy FT-IR was used to determine the presence of the active substance and the compounds used in microencapsulation in the system and to observe the spectrum change of the active substance in microcapsules.

 In our study, cabbage plant extract containing the active ingredient S-methylmethionine vitamin U was successfully microencapsulated by complex coacervation method using two different natural polymeric wall materials consisting of Gelatin-Gum Arabic GE-GA and Gelatin-Sodium alginate GE-SA. A response surface methodology RSM was used to optimize the encapsulation efficiency conditions. The encapsulation efficiency of the microencapsulated cabbage extract was investigated using different polymers in terms of two variables: the amount of core material g and the amount of crosslinker mL. The highest yields obtained as a result of the experiments were 67.72 for gelatin-gum arabic and 54.68 for gelatin-sodium alginate. The morphological structures of the microcapsules with the highest efficiency were examined by optical microscope and scanning electron microscope SEM. The Fourier transform infrared spectroscopy FT-IR was used to determine the presence of the active substance and the compounds used in microencapsulation in the system and to observe the spectrum change of the active substance in microcapsules.

 In our study, cabbage plant extract containing the active ingredient S-methylmethionine vitamin U was successfully microencapsulated by complex coacervation method using two different natural polymeric wall materials consisting of Gelatin-Gum Arabic GE-GA and Gelatin-Sodium alginate GE-SA. A response surface methodology RSM was used to optimize the encapsulation efficiency conditions. The encapsulation efficiency of the microencapsulated cabbage extract was investigated using different polymers in terms of two variables: the amount of core material g and the amount of crosslinker mL. The highest yields obtained as a result of the experiments were 67.72 for gelatin-gum arabic and 54.68 for gelatin-sodium alginate. The morphological structures of the microcapsules with the highest efficiency were examined by optical microscope and scanning electron microscope SEM. The Fourier transform infrared spectroscopy FT-IR was used to determine the presence of the active substance and the compounds used in microencapsulation in the system and to observe the spectrum change of the active substance in microcapsules.

 Çalışmamızda S-metilmetiyonin vitamin U etken maddesini içeren lahana bitki ekstraktının, Jelatin-Arap zamkı GE-GA ve Jelatin-Sodyum aljinattanGE-SA oluşan iki farklı doğal polimerik duvar materyali kullanılarak kompleks koaservasyon yöntemiyle başarılı bir şekilde mikroenkapsüle edilmiştir. Kapsülleme verimliliği koşulları optimize etmek için bir yanıt yüzeyi metodolojisi RSM kullanılmıştır. Mikrokapsüllenmiş lahana ekstraktının kapsülleme verimliliği farklı polimerler kullanılarak iki değişken açısından araştırılmıştır: çekirdek madde miktarıg ve çapraz bağlayıcı miktarı mL. Deneyler sonucunda elde edilen en yüksek verimler jelatin- arap zamkı için 67,72 ve jelatin-sodyum aljinat için de 54,68 olarak bulunmuştur. En yüksek verimlilik elde edilen mikrokapsüllerin morfolojik yapıları optik mikroskop ve taramalı elektron mikroskobu SEM ile incelenmiştir. Etken maddenin ve mikrokapsülasyonda kullanılan bileşiklerin sistemdeki varlığının belirlenmesi ve elde edilen mikrokapsüllerde etken maddenin spektrum değişiminin gözlenmesi için Fourier dönüşümü kızılötesi spektroskopi FT-IR kullanılmıştır.

Makale detayları

Microencapsulation and Characterization Studies of Brassica oleracea var. capitata L. (Cabbage) Plant Extract Using Response Surface Methodology

Yazarlar:

Elif Köksal | Fethiye Göde

Yayıncı:

Afyon Kocatepe University

Ana Başlıklar:

Mühendislik

Dergi:

Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.24 Issue 1, pp.14-22

Belge Tipi:

Makale

Yayın Tarihi:

2/2024

Belge Dili:

Türkçe

Document ID (Org No.):

2001312333

pISSN:

2149-3367

S-metilmetiyonin (vitamin U)

Microencapsulation

Response Surface Methodology

Encapsulation EfficiencyS-metilmetiyonin (vitamin U)

Mikroenkapsülasyon

Yanıt Yüzey Metodolojisi

Enkapsülasyon Verimliliği

Sayı

Makale detayları

Yazarlar: Elif Köksal | Fethiye Göde

Yayıncı: Afyon Kocatepe University

Ana Başlıklar: Mühendislik

Dergi: Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.24 Issue 1, pp.14-22

Belge Tipi: Makale

Yayın Tarihi: 2/2024

Belge Dili: Türkçe

Document ID (Org No.): 2001312333

pISSN: 2149-3367

Sayı

Yazarlar:

Elif Köksal | Fethiye Göde

Yayıncı:

Afyon Kocatepe University

Ana Başlıklar:

Mühendislik

Dergi:

Afyon Kocatepe Üniversitesi Fen Ve Mühendislik Bilimleri Dergisi Vol.24 Issue 1, pp.14-22

Belge Tipi:

Makale

Yayın Tarihi:

2/2024

Belge Dili:

Türkçe

Document ID (Org No.):

2001312333

pISSN:

2149-3367