Microencapsulation of Hemp Oil with Gelatin and Sodium Alginate Polymers and  Investigation of Release Properties

Okan Bayram; Fethiye Göde

Makale detayları

Microencapsulation of Hemp Oil with Gelatin and Sodium Alginate Polymers and Investigation of Release Properties

Yazarlar:

Okan Bayram | Fethiye Göde

Yayıncı:

Süleyman Demirel University

Ana Başlıklar:

Mühendislik

Dergi:

Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.27 Issue 3, pp.527-532

Belge Tipi:

Makale

Yayın Tarihi:

12/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001305708

pISSN:

1308-6529

Anahtar kelimeler:

Özet:

 Hemp oil is an oil used for different purposes around the world. In this study, hemp oil with different properties was microencapsulated by complex coacervation method in an experiment set formed with gelatin GE and sodium alginate ALG. Stirring speed, temperature and surfactant concentration were chosen as input factors and the relationship between percent encapsulation efficiency EE was investigated. The obtained results were optimized to maximize and the release properties in hexane medium were investigated. In the results obtained, the p value of the lack-of-fit was found to be 0.060. Since p0.050, the data matches the model created. Maximize optimized results were calculated as 63.491 at 1460.310 rpm stirring speed, 56.897  temperature and 0.827 wv surfactant concentration, and it was found to be 62.780 in the experiment. Obtained microcapsules were characterized by FT-IR, optical microscope and SEM devices. When the optical microscope images were examined, it was determined that the microcapsules were smooth and round in shape.

 Hemp oil is an oil used for different purposes around the world. In this study, hemp oil with different properties was microencapsulated by complex coacervation method in an experiment set formed with gelatin GE and sodium alginate ALG. Stirring speed, temperature and surfactant concentration were chosen as input factors and the relationship between percent encapsulation efficiency EE was investigated. The obtained results were optimized to maximize and the release properties in hexane medium were investigated. In the results obtained, the p value of the lack-of-fit was found to be 0.060. Since p0.050, the data matches the model created. Maximize optimized results were calculated as 63.491 at 1460.310 rpm stirring speed, 56.897  temperature and 0.827 wv surfactant concentration, and it was found to be 62.780 in the experiment. Obtained microcapsules were characterized by FT-IR, optical microscope and SEM devices. When the optical microscope images were examined, it was determined that the microcapsules were smooth and round in shape.

 Hemp oil is an oil used for different purposes around the world. In this study, hemp oil with different properties was microencapsulated by complex coacervation method in an experiment set formed with gelatin GE and sodium alginate ALG. Stirring speed, temperature and surfactant concentration were chosen as input factors and the relationship between percent encapsulation efficiency EE was investigated. The obtained results were optimized to maximize and the release properties in hexane medium were investigated. In the results obtained, the p value of the lack-of-fit was found to be 0.060. Since p0.050, the data matches the model created. Maximize optimized results were calculated as 63.491 at 1460.310 rpm stirring speed, 56.897  temperature and 0.827 wv surfactant concentration, and it was found to be 62.780 in the experiment. Obtained microcapsules were characterized by FT-IR, optical microscope and SEM devices. When the optical microscope images were examined, it was determined that the microcapsules were smooth and round in shape.

 Kenevir yağı dünyada farklı amaçlar için kullanılan bir yağdır. Farklı özelliklere sahip olan kenevir yağı bu çalışmada jelatin JE ve sodyum aljinat ALJ ile oluşturulan bir deney setinde kompleks koaservasyon yöntemiyle mikroenkapsüle edilmiştir. Karıştırma hızı, sıcaklık ve surfaktan derişimi giriş faktörleri olarak seçilmiş ve yüzde enkapsülasyon verimi EV ile arasındaki ilişki incelenmiştir. Elde edilen sonuçlar maksimize olarak optimize edilmiş ve hekzan ortamında salınım özellikleri incelenmiştir. Elde edilen sonuçlarda model uyumsuzluğunun p değeri 0,060 bulunmuştur. p0,050 olduğu için oluşturulan model ile veri uyuşmaktadır. Maksimize olarak optimize edilen sonuçlar 1460,310 rpm karıştırma hızı, 56,897  sıcaklık ve 0,827 ah surfaktan derişiminde verim değeri 63,491 hesaplanmış ve yapılan deneyde 62,780 olarak bulunmuştur. Elde edilen mikrokapsüller FT-IR, optik mikroskop ve SEM cihazları ile karakterize edilmiştir. Optik mikroskop görüntüleri incelendiğinde mikrokapsüllerin düzgün, yuvarlak şeklinde olduğunu belirlenmiştir.

Makale detayları

Microencapsulation of Hemp Oil with Gelatin and Sodium Alginate Polymers and Investigation of Release Properties

Yazarlar:

Okan Bayram | Fethiye Göde

Yayıncı:

Süleyman Demirel University

Ana Başlıklar:

Mühendislik

Dergi:

Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.27 Issue 3, pp.527-532

Belge Tipi:

Makale

Yayın Tarihi:

12/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001305708

pISSN:

1308-6529

Gelatine

Sodium Alginate

Hemp Oil

Encapsulation

Release

Experimental DesignKenevir yağı

Enkapsülasyon

Salınım

Jelatin

Sodyum Aljinat

Deney Tasarımı

Sayı

Makale detayları

Yazarlar: Okan Bayram | Fethiye Göde

Yayıncı: Süleyman Demirel University

Ana Başlıklar: Mühendislik

Dergi: Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.27 Issue 3, pp.527-532

Belge Tipi: Makale

Yayın Tarihi: 12/2023

Belge Dili: Türkçe

Document ID (Org No.): 2001305708

pISSN: 1308-6529

Sayı

Yazarlar:

Okan Bayram | Fethiye Göde

Yayıncı:

Süleyman Demirel University

Ana Başlıklar:

Mühendislik

Dergi:

Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.27 Issue 3, pp.527-532

Belge Tipi:

Makale

Yayın Tarihi:

12/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001305708

pISSN:

1308-6529