Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γγ\gamma -Fe22_{2}O33_{3} nanoparticles for preconcentration and determination of   Al(III) in water and food samples

Sadin ÖZDEMİR; Mustafa Serkan YALÇIN; Ersin KILINÇ; Mustafa SOYLAK

Makale detayları

Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γγ\gamma -Fe22_{2}O33_{3} nanoparticles for preconcentration and determination of Al(III) in water and food samples

Yazarlar:

Sadin ÖZDEMİR | Mustafa Serkan YALÇIN | Ersin KILINÇ | Mustafa SOYLAK

Yayıncı:

TUBITAK

Dergi:

Turkish Journal of Chemistry 2019 Vol.43 Issue 5, pp.1217-1228

Belge Tipi:

Makale

Yayın Tarihi:

9/2019

Belge Dili:

İngilizce

Document ID (Org No.):

2000725558

Sıklık:

İki Aylık

eISSN:

1303-6130

pISSN:

1300-0527

Özet:

 

A method for preconcentration of Al(III) prior to its determination by   inductively coupled plasma-optical emission spectrometry (ICP-OES) was   developed because the sensitivity of ICP-OES is insufficient for trace-level   measurement of Al(III). The method is based on the use of Coriolus versicolor}-immobilized γγ\gamma -Fe22_{2}O33_{3}   magnetic nanoparticles as a solid   phase sorbent. The best experimental conditions were found as pH 6.0, 2.0   mL/min flow rate, 100 mg amount of C. versicoloron 150 mg of γγ\gamma -Fe22_{2}O33_{3}   nanoparticles, and 500 mL of sample volume. The Al(III) absorbed on biosorbent was eluted with 5.0 mL of 1.0 mol/L HCl. Limit of detection,   limit of quantitation, linear range, correlation coefficient, relative   standard deviation, and preconcentration factor were achieved as 0.03 ng/mL,   0.11 ng/mL, 0.2 to 20 ng/mL, 0.9994, 3%, and 100, respectively. Al(III)   was preconcentrated in different water and food samples after successful   results were achieved in the case of certified reference samples.

Makale detayları

Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γγ\gamma -Fe22_{2}O33_{3} nanoparticles for preconcentration and determination of Al(III) in water and food samples

Yazarlar: Sadin ÖZDEMİR | Mustafa Serkan YALÇIN | Ersin KILINÇ | Mustafa SOYLAK

Yayıncı: TUBITAK

Dergi: Turkish Journal of Chemistry 2019 Vol.43 Issue 5, pp.1217-1228

Belge Tipi: Makale

Yayın Tarihi: 9/2019

Belge Dili: İngilizce

Document ID (Org No.): 2000725558

Sıklık: İki Aylık

eISSN: 1303-6130

pISSN: 1300-0527

Sayı

Yazarlar:

Sadin ÖZDEMİR | Mustafa Serkan YALÇIN | Ersin KILINÇ | Mustafa SOYLAK

Yayıncı:

TUBITAK

Dergi:

Turkish Journal of Chemistry 2019 Vol.43 Issue 5, pp.1217-1228

Belge Tipi:

Makale

Yayın Tarihi:

9/2019

Belge Dili:

İngilizce

Document ID (Org No.):

2000725558

Sıklık:

İki Aylık

eISSN:

1303-6130

pISSN:

1300-0527