Preparation and Characterisation of LAITP/PVDF Composite Solid Electrolyte for Lithium Battery

Fatih Öksüzoğlu; Osman Murat Özkendir; Şule Ateş

Makale detayları

Preparation and Characterisation of LAITP/PVDF Composite Solid Electrolyte for Lithium Battery

Yazarlar:

Fatih Öksüzoğlu | Osman Murat Özkendir | Şule Ateş

Yayıncı:

Gazi University

Ana Başlıklar:

Solid State Chemistry | Electrical Energy Storage

Dergi:

Gazi University Journal of Science Vol.38 Issue 3, pp.1449-1460

Belge Tipi:

Makale

Yayın Tarihi:

1/2025

Belge Dili:

İngilizce

Document ID (Org No.):

2001356585

pISSN:

2147-1762

Anahtar kelimeler:

Özet:

 This study investigates the potential of LAITPPVDF composite electrolytes to improve the safety and performance of lithium-ion batteries. The study focuses on the synthesis and characterization of composite solid electrolyte consisting of indium-doped lithium aluminum titanium phosphate LAITP ceramic material and LiClO4 salt with polyvinylidene fluoride PVDF as the polymer matrix. The LAITP ceramic, synthesized via solid-state synthesis, demonstrates high ionic conductivity, thermal stability, and mechanical robustness. PVDF provides electrochemical and thermal stability to the composite. The composite electrolytes were prepared by integrating LAITP into the PVDF matrix through the solution casting method. Various characterization methods were employed to assess the properties of the resulting composite. X-ray diffraction XRD was used to examine the crystal structure, while scanning electron microscopy SEM provided insights into the morphological features. Ionic conductivity measurements were conducted using electrochemical impedance spectroscopy EIS, enabling an evaluation of the composites electrochemical performance. The LAITP-reinforced PVDF-based composite solid electrolyte exhibited an ionic conductivity of 1.7  105 S cm1 at room temperature.

 This study investigates the potential of LAITPPVDF composite electrolytes to improve the safety and performance of lithium-ion batteries. The study focuses on the synthesis and characterization of composite solid electrolyte consisting of indium-doped lithium aluminum titanium phosphate LAITP ceramic material and LiClO4 salt with polyvinylidene fluoride PVDF as the polymer matrix. The LAITP ceramic, synthesized via solid-state synthesis, demonstrates high ionic conductivity, thermal stability, and mechanical robustness. PVDF provides electrochemical and thermal stability to the composite. The composite electrolytes were prepared by integrating LAITP into the PVDF matrix through the solution casting method. Various characterization methods were employed to assess the properties of the resulting composite. X-ray diffraction XRD was used to examine the crystal structure, while scanning electron microscopy SEM provided insights into the morphological features. Ionic conductivity measurements were conducted using electrochemical impedance spectroscopy EIS, enabling an evaluation of the composites electrochemical performance. The LAITP-reinforced PVDF-based composite solid electrolyte exhibited an ionic conductivity of 1.7  105 S cm1 at room temperature.

 This study investigates the potential of LAITPPVDF composite electrolytes to improve the safety and performance of lithium-ion batteries. The study focuses on the synthesis and characterization of composite solid electrolyte consisting of indium-doped lithium aluminum titanium phosphate LAITP ceramic material and LiClO4 salt with polyvinylidene fluoride PVDF as the polymer matrix. The LAITP ceramic, synthesized via solid-state synthesis, demonstrates high ionic conductivity, thermal stability, and mechanical robustness. PVDF provides electrochemical and thermal stability to the composite. The composite electrolytes were prepared by integrating LAITP into the PVDF matrix through the solution casting method. Various characterization methods were employed to assess the properties of the resulting composite. X-ray diffraction XRD was used to examine the crystal structure, while scanning electron microscopy SEM provided insights into the morphological features. Ionic conductivity measurements were conducted using electrochemical impedance spectroscopy EIS, enabling an evaluation of the composites electrochemical performance. The LAITP-reinforced PVDF-based composite solid electrolyte exhibited an ionic conductivity of 1.7  105 S cm1 at room temperature.

 This study investigates the potential of LAITPPVDF composite electrolytes to improve the safety and performance of lithium-ion batteries. The study focuses on the synthesis and characterization of composite solid electrolyte consisting of indium-doped lithium aluminum titanium phosphate LAITP ceramic material and LiClO4 salt with polyvinylidene fluoride PVDF as the polymer matrix. The LAITP ceramic, synthesized via solid-state synthesis, demonstrates high ionic conductivity, thermal stability, and mechanical robustness. PVDF provides electrochemical and thermal stability to the composite. The composite electrolytes were prepared by integrating LAITP into the PVDF matrix through the solution casting method. Various characterization methods were employed to assess the properties of the resulting composite. X-ray diffraction XRD was used to examine the crystal structure, while scanning electron microscopy SEM provided insights into the morphological features. Ionic conductivity measurements were conducted using electrochemical impedance spectroscopy EIS, enabling an evaluation of the composites electrochemical performance. The LAITP-reinforced PVDF-based composite solid electrolyte exhibited an ionic conductivity of 1.7  105 S cm1 at room temperature.

Makale detayları

Preparation and Characterisation of LAITP/PVDF Composite Solid Electrolyte for Lithium Battery

Yazarlar:

Fatih Öksüzoğlu | Osman Murat Özkendir | Şule Ateş

Yayıncı:

Gazi University

Ana Başlıklar:

Solid State Chemistry | Electrical Energy Storage

Dergi:

Gazi University Journal of Science Vol.38 Issue 3, pp.1449-1460

Belge Tipi:

Makale

Yayın Tarihi:

1/2025

Belge Dili:

İngilizce

Document ID (Org No.):

2001356585

pISSN:

2147-1762

LATP ceramic electrolyte

PVDF polymer electrolyte

Composite electrolyte

Sayı

Makale detayları

Preparation and Characterisation of LAITP/PVDF Composite Solid Electrolyte for Lithium Battery

Yazarlar: Fatih Öksüzoğlu | Osman Murat Özkendir | Şule Ateş

Yayıncı: Gazi University

Ana Başlıklar: Solid State Chemistry | Electrical Energy Storage

Dergi: Gazi University Journal of Science Vol.38 Issue 3, pp.1449-1460

Belge Tipi: Makale

Yayın Tarihi: 1/2025

Belge Dili: İngilizce

Document ID (Org No.): 2001356585

pISSN: 2147-1762

LATP ceramic electrolyte

PVDF polymer electrolyte

Composite electrolyte

Sayı

Yazarlar:

Fatih Öksüzoğlu | Osman Murat Özkendir | Şule Ateş

Yayıncı:

Gazi University

Ana Başlıklar:

Solid State Chemistry | Electrical Energy Storage

Dergi:

Gazi University Journal of Science Vol.38 Issue 3, pp.1449-1460

Belge Tipi:

Makale

Yayın Tarihi:

1/2025

Belge Dili:

İngilizce

Document ID (Org No.):

2001356585

pISSN:

2147-1762