Investigation of Different Molecular Weights Chitosan Added Hydroxyapatite/Chitosan Biocomposite Coatings

Tuncay Dilsizoğlu; İsmail Hakki Karahan; Ali Tozar

Makale detayları

Investigation of Different Molecular Weights Chitosan Added Hydroxyapatite/Chitosan Biocomposite Coatings

Yazarlar:

Tuncay Dilsizoğlu | İsmail Hakki Karahan | Ali Tozar

Yayıncı:

Igdir University

Ana Başlıklar:

Metroloji | Uygulamalı ve Endüstriyel Fizik

Dergi:

Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.13 Issue 3, pp.1703-1712

Belge Tipi:

Makale

Yayın Tarihi:

1/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001296817

pISSN:

2536-4618

Anahtar kelimeler:

Özet:

 Which is the nearest of the bone structure of calcium phosphate rate HAp, Ca10PO46OH2 is hydroxyapatite. However, it is known that the mechanical properties of hydroxyapatite HAp such as strength and hardness are increased with polymer additives. Chitosan CTS was used as the polymer due to its low toxicity and high biocompatibility properties. Two types of chitosan were used while making HApCTS coatings. Medium molecular weight MMW and high molecular weight HMW. The effect of HApCTS biocomposite coatings by doping with medium and high molecular weight chitosan was investigated. The coatings were produced by the ultrasonic assisted electrophoretic method. Their crystallographic and morphological structures were examined by FT-IR, XRD and SEM. The structure of the sample become more homogeneous as the high molecular weight chitosan value increased.

 Which is the nearest of the bone structure of calcium phosphate rate HAp, Ca10PO46OH2 is hydroxyapatite. However, it is known that the mechanical properties of hydroxyapatite HAp such as strength and hardness are increased with polymer additives. Chitosan CTS was used as the polymer due to its low toxicity and high biocompatibility properties. Two types of chitosan were used while making HApCTS coatings. Medium molecular weight MMW and high molecular weight HMW. The effect of HApCTS biocomposite coatings by doping with medium and high molecular weight chitosan was investigated. The coatings were produced by the ultrasonic assisted electrophoretic method. Their crystallographic and morphological structures were examined by FT-IR, XRD and SEM. The structure of the sample become more homogeneous as the high molecular weight chitosan value increased.

 Which is the nearest of the bone structure of calcium phosphate rate HAp, Ca10PO46OH2 is hydroxyapatite. However, it is known that the mechanical properties of hydroxyapatite HAp such as strength and hardness are increased with polymer additives. Chitosan CTS was used as the polymer due to its low toxicity and high biocompatibility properties. Two types of chitosan were used while making HApCTS coatings. Medium molecular weight MMW and high molecular weight HMW. The effect of HApCTS biocomposite coatings by doping with medium and high molecular weight chitosan was investigated. The coatings were produced by the ultrasonic assisted electrophoretic method. Their crystallographic and morphological structures were examined by FT-IR, XRD and SEM. The structure of the sample become more homogeneous as the high molecular weight chitosan value increased.

 Kemiğin yapısına en yakın olan kalsiyum fosfat; Ca10PO46OH2 oranının olduğu hidroksiapatittir HA. Ancak polimer katkısıyla hidroksiapatitin HA mukavemet ve sertlik gibi mekanik özelliklerinin arttırıldığı bilinmektedir. Düşük toksiklik ve yüksek biyouyumluluk özelliklerinden dolayı kitosan CTS polimer olarak kullanıldı. HACTS kaplamaları yapılırken orta moleküler ağırlıklı MMW ve yüksek moleküler ağırlıklı HMW olmak üzere iki farklı moleküler ağırlıklı kitosan kullanıldı. Orta ve yüksek moleküler ağırlıklı kitosan katkılanarak HACTS biyokompozit kaplamalarının etkisi incelendi. Kaplamalar ultasonik destekli elektroforetik yöntemle üretildi. Kristalografik, morfolojik yapıları FT-IR, XRD ve SEM ile incelendi. Yüksek moleküler ağırlıklı kitosan değeri arttıkça numunenin yapısının daha homojen olduğu belirlendi.

Makale detayları

Investigation of Different Molecular Weights Chitosan Added Hydroxyapatite/Chitosan Biocomposite Coatings

Yazarlar:

Tuncay Dilsizoğlu | İsmail Hakki Karahan | Ali Tozar

Yayıncı:

Igdir University

Ana Başlıklar:

Metroloji | Uygulamalı ve Endüstriyel Fizik

Dergi:

Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.13 Issue 3, pp.1703-1712

Belge Tipi:

Makale

Yayın Tarihi:

1/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001296817

pISSN:

2536-4618

Hydroxypatite

Chitosan

Biocomposite

Ultrasonic

Electrophoretic depositionHidroksiapatit

Kitosan

Biyokompozit

Ultrasonik

Elektroforetik depolama

Sayı

Makale detayları

Yazarlar: Tuncay Dilsizoğlu | İsmail Hakki Karahan | Ali Tozar

Yayıncı: Igdir University

Ana Başlıklar: Metroloji | Uygulamalı ve Endüstriyel Fizik

Dergi: Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.13 Issue 3, pp.1703-1712

Belge Tipi: Makale

Yayın Tarihi: 1/2023

Belge Dili: Türkçe

Document ID (Org No.): 2001296817

pISSN: 2536-4618

Sayı

Yazarlar:

Tuncay Dilsizoğlu | İsmail Hakki Karahan | Ali Tozar

Yayıncı:

Igdir University

Ana Başlıklar:

Metroloji | Uygulamalı ve Endüstriyel Fizik

Dergi:

Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.13 Issue 3, pp.1703-1712

Belge Tipi:

Makale

Yayın Tarihi:

1/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001296817

pISSN:

2536-4618