Preparation of Cerium Oxide Nanoparticles: An Efficient Catalyst to the Synthesis of  Dimeric Disulphide Schiff Bases

Sefa Durmuş; Aslıhan Dalmaz; Mesut Özdinçer; Sezen Sivrikaya

Makale detayları

Preparation of Cerium Oxide Nanoparticles: An Efficient Catalyst to the Synthesis of Dimeric Disulphide Schiff Bases

Yazarlar:

Sefa Durmuş | Aslıhan Dalmaz | Mesut Özdinçer | Sezen Sivrikaya

Yayıncı:

Celal Bayar University

Ana Başlıklar:

Uygulamalı fizik

Dergi:

Celal Bayar University Journal of Science 2017 Vol.13 Issue 1, pp.25-30

Belge Tipi:

Makale

Yayın Tarihi:

3/2017

Belge Dili:

Türkçe

Document ID (Org No.):

2000706611

Sıklık:

Üç Aylık

eISSN:

1305-1385

pISSN:

1305-130X

Özet:

 


Dimeric disulphide Schiff bases were synthesized via reactions of 2-aminophenyl disulphide with various aromatic
aldehydes under reflux and prepared nano‐sized
cerium oxide as catalyst. It observed that, when nanocatalyst were used, the
catalyst could be reduced the reaction time and increased yields compared with
the none-catalyst conditions. Moreover, the CeO2 nanocatalyst were easy
preparation, non-hazardous, eco-friendliness and low cost. The morphological features
of CeO2 nanocatalyst were characterized by X-ray diffraction (XRD),
scanning electron microscopy (SEM), energy dispersive X-ray (EDX), but also ligand
structures were investigated some techniques such as fourier transform infrared
(FT-IR), nuclear magnetic resonance (NMR) spectroscopy and thermogravimetric
analysis (TGA) / differential thermal analysis (DTA). 



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Makale detayları

Preparation of Cerium Oxide Nanoparticles: An Efficient Catalyst to the Synthesis of Dimeric Disulphide Schiff Bases

Yazarlar: Sefa Durmuş | Aslıhan Dalmaz | Mesut Özdinçer | Sezen Sivrikaya

Yayıncı: Celal Bayar University

Ana Başlıklar: Uygulamalı fizik

Dergi: Celal Bayar University Journal of Science 2017 Vol.13 Issue 1, pp.25-30

Belge Tipi: Makale

Yayın Tarihi: 3/2017

Belge Dili: Türkçe

Document ID (Org No.): 2000706611

Sıklık: Üç Aylık

eISSN: 1305-1385

pISSN: 1305-130X

Sayı

Yazarlar:

Sefa Durmuş | Aslıhan Dalmaz | Mesut Özdinçer | Sezen Sivrikaya

Yayıncı:

Celal Bayar University

Ana Başlıklar:

Uygulamalı fizik

Dergi:

Celal Bayar University Journal of Science 2017 Vol.13 Issue 1, pp.25-30

Belge Tipi:

Makale

Yayın Tarihi:

3/2017

Belge Dili:

Türkçe

Document ID (Org No.):

2000706611

Sıklık:

Üç Aylık

eISSN:

1305-1385

pISSN:

1305-130X