Determination of Mineral Matter in Some Molasses of Giresun Region by ICP-MS and IC System

Berna Öztürk; Zuhal Yolcu; Elif Apaydın; Murat Yolcu

Makale detayları

Determination of Mineral Matter in Some Molasses of Giresun Region by ICP-MS and IC System

Yazarlar:

Berna Öztürk | Zuhal Yolcu | Elif Apaydın | Murat Yolcu

Yayıncı:

Aydin Adnan Menderes University

Ana Başlıklar:

Gıda Mühendisliği

Dergi:

Adnan Menderes Üniversitesi Ziraat Fakültesi Dergisi Vol.20 Issue 1, pp.117-125

Belge Tipi:

Makale

Yayın Tarihi:

6/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001295686

pISSN:

1304-7787

Anahtar kelimeler:

Özet:

 In this study, Ion Chromatography IC system was used to determine the mineral content, and Inductively Coupled Plasma Mass Spectrometry ICP-MS was used to determine the heavy metal content of six different molasses varieties, namely taflan, pear, black grape, white grape, kiwi and apple purchased from various neighborhood markets of Giresun province. Quantitative analyses of some common anions fluoride, chloride, bromide, nitrite, nitrate, phosphate, sulfate and cations lithium, sodium, ammonium, potassium, magnesium and calcium were performed with the IC system, while heavy metals of aluminum, chromium, iron, copper and zinc and mineral substances of lithium, sodium, magnesium and calcium were analyzed with the ICP-MS system. According to data, when the mineral content of molasses was evaluated, the highest amount of potassium K pear molasses; 11979.10.7 followed by calcium Ca taflan molasses; 1213.70.4, magnesium Mg taflan molasses; 559.30.01, sodium Na black grape molasses; 133.30.03 was detected in the IC system. In the ICP-MS system, the highest amount of calcium Ca taflan molasses; 1771.177.9, followed by magnesium Mg taflan molasses; 909.314.1 and sodium Na taflan molasses; 122.48.7, respectively. A two-sided t-test at 95 confidence level was applied to the results of the mineral items common to both systems and no significant difference was found.

 In this study, Ion Chromatography IC system was used to determine the mineral content, and Inductively Coupled Plasma Mass Spectrometry ICP-MS was used to determine the heavy metal content of six different molasses varieties, namely taflan, pear, black grape, white grape, kiwi and apple purchased from various neighborhood markets of Giresun province. Quantitative analyses of some common anions fluoride, chloride, bromide, nitrite, nitrate, phosphate, sulfate and cations lithium, sodium, ammonium, potassium, magnesium and calcium were performed with the IC system, while heavy metals of aluminum, chromium, iron, copper and zinc and mineral substances of lithium, sodium, magnesium and calcium were analyzed with the ICP-MS system. According to data, when the mineral content of molasses was evaluated, the highest amount of potassium K pear molasses; 11979.10.7 followed by calcium Ca taflan molasses; 1213.70.4, magnesium Mg taflan molasses; 559.30.01, sodium Na black grape molasses; 133.30.03 was detected in the IC system. In the ICP-MS system, the highest amount of calcium Ca taflan molasses; 1771.177.9, followed by magnesium Mg taflan molasses; 909.314.1 and sodium Na taflan molasses; 122.48.7, respectively. A two-sided t-test at 95 confidence level was applied to the results of the mineral items common to both systems and no significant difference was found.

 In this study, Ion Chromatography IC system was used to determine the mineral content, and Inductively Coupled Plasma Mass Spectrometry ICP-MS was used to determine the heavy metal content of six different molasses varieties, namely taflan, pear, black grape, white grape, kiwi and apple purchased from various neighborhood markets of Giresun province. Quantitative analyses of some common anions fluoride, chloride, bromide, nitrite, nitrate, phosphate, sulfate and cations lithium, sodium, ammonium, potassium, magnesium and calcium were performed with the IC system, while heavy metals of aluminum, chromium, iron, copper and zinc and mineral substances of lithium, sodium, magnesium and calcium were analyzed with the ICP-MS system. According to data, when the mineral content of molasses was evaluated, the highest amount of potassium K pear molasses; 11979.10.7 followed by calcium Ca taflan molasses; 1213.70.4, magnesium Mg taflan molasses; 559.30.01, sodium Na black grape molasses; 133.30.03 was detected in the IC system. In the ICP-MS system, the highest amount of calcium Ca taflan molasses; 1771.177.9, followed by magnesium Mg taflan molasses; 909.314.1 and sodium Na taflan molasses; 122.48.7, respectively. A two-sided t-test at 95 confidence level was applied to the results of the mineral items common to both systems and no significant difference was found.

 Bu çalışmada, Giresun ilinin çeşitli semt pazarlarından satın alınan taflan, armut, kara üzüm, beyaz üzüm, kivi ve elma olmak üzere altı farklı pekmez çeşidinin mineral madde içeriklerini belirlemek için İyon Kromatografi IC sistemi ve ağır metal içeriklerini belirlemek için İndüktif Eşleşmiş Plazma Kütle Spektrometresi ICP-MS kullanılmıştır. IC sistemi ile bazı yaygın anyonların florür, klorür, bromür, nitrit, nitrat, fosfat, sülfat ve katyonların lityum, sodyum, amonyum, potasyum, magnezyum ve kalsiyum kantitatif analizleri yapılırken, ICP-MS sistemi ile alüminyum, krom, demir, bakır ve çinko ağır metalleri ve lityum, sodyum, magnezyum, kalsiyum mineral madde analizleri yapılmıştır. Bu verilere göre pekmezlerin mineral madde içerikleri değerlendirildiğinde, IC sisteminde en fazla miktarda potasyum K armut pekmezi; 11979.10.7 daha sonra sırasıyla kalsiyum Ca taflan pekmezi; 1213.70.4, magnezyum Mg taflan pekmezi; 559.30.01 ve sodyum Na kara üzüm pekmezi; 133.30.03 iyonları tespit edilmiştir. ICP-MS sisteminde ise en fazla kalsiyum Ca taflan pekmezi; 1771.177.9, daha sonra sırasıyla magnezyum Mg taflan pekmezi; 909.314.1 ve sodyum Na taflan pekmezi; 122.48.7 tespit edilmiştir. Her iki sistemde ortak olarak belirlenen mineral madde sonuçlarına,  95 güven seviyesinde çift taraflı t testi uygulanmış ve anlamlı fark bulunmamıştır.

Makale detayları

Determination of Mineral Matter in Some Molasses of Giresun Region by ICP-MS and IC System

Yazarlar:

Berna Öztürk | Zuhal Yolcu | Elif Apaydın | Murat Yolcu

Yayıncı:

Aydin Adnan Menderes University

Ana Başlıklar:

Gıda Mühendisliği

Dergi:

Adnan Menderes Üniversitesi Ziraat Fakültesi Dergisi Vol.20 Issue 1, pp.117-125

Belge Tipi:

Makale

Yayın Tarihi:

6/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001295686

pISSN:

1304-7787

Molasses

mineral substance

Inductively Coupled Plasma-Mass Spectrometer (ICP-MS)

Ion Chromatography (IC)Pekmez

Mineral madde

İndüktif Eşleşmiş Plazma Kütle Spektrometresi (ICP-MS)

İyon Kromatografisi (IC)

Sayı

Makale detayları

Yazarlar: Berna Öztürk | Zuhal Yolcu | Elif Apaydın | Murat Yolcu

Yayıncı: Aydin Adnan Menderes University

Ana Başlıklar: Gıda Mühendisliği

Dergi: Adnan Menderes Üniversitesi Ziraat Fakültesi Dergisi Vol.20 Issue 1, pp.117-125

Belge Tipi: Makale

Yayın Tarihi: 6/2023

Belge Dili: Türkçe

Document ID (Org No.): 2001295686

pISSN: 1304-7787

Sayı

Yazarlar:

Berna Öztürk | Zuhal Yolcu | Elif Apaydın | Murat Yolcu

Yayıncı:

Aydin Adnan Menderes University

Ana Başlıklar:

Gıda Mühendisliği

Dergi:

Adnan Menderes Üniversitesi Ziraat Fakültesi Dergisi Vol.20 Issue 1, pp.117-125

Belge Tipi:

Makale

Yayın Tarihi:

6/2023

Belge Dili:

Türkçe

Document ID (Org No.):

2001295686

pISSN:

1304-7787